HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 70636802, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | HCID 70637887 | HCID 70637887 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 70636802 | HCID 70636802 | — |
Reaction Steps
1 g of 2-keto-1,2,3,4,10,14b-hexahydro-pyridino[ 1,2-a] -dibenzo[c,f]-azepine is dissolved in 100 ml of ethanol, after which 10 ml of methylamine and 200 mg of palladium (10%) on charcoal are added. Then hydrogen is passed through this mixture until no hydrogen is absorbed any longer.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04054572 |
| Source dataset | uspto-grants-1977_10 |
| ORD ID | ord-5f188c07518941e78f7cf37727122b26 |
| Source note | uspto-grants-1977_10 |