HCID 70636802, compound → HCID 70636775, compound

HRID 972948Notes

Reaction equation

HRID 972948 reaction equation
C[NH:2][CH:3]1[CH2:21][CH2:20][N:6]2[C:7]3[CH:19]=[CH:18][CH:17]=[CH:16][C:8]=3[CH2:9][C:10]3[CH:15]=[CH:14][CH:13]=[CH:12][C:11]=3[CH:5]2[CH2:4]1>CO.CC(C)=O>[NH2:2][CH:3]1[CH2:21][CH2:20][N:6]2[C:7]3[CH:19]=[CH:18][CH:17]=[CH:16][C:8]=3[CH2:9][C:10]3[CH:15]=[CH:14][CH:13]=[CH:12][C:11]=3[CH:5]2[CH2:4]1

Participants

3

Reactant 1

HCID 70636802HCID 70636802, compound

Product 1

HCID 70636775HCID 70636775, compound

Reagents, catalysts & solvents 1

HCID 21894497Aceton-methanolSolvent

Procedure

2-methylamino-1,2,3,4,10,14b-hexahydro-pyridino[1,2-a]-dibenzo[c,f]-azepine, oil; Rf in methanol:acetone (9:1) = 0.35 on SiO2.

Sources & evidence

ORD record
ord-6199cdc3372a454f931c1c61d4095b72
Source dataset
uspto-grants-1977_10
Patent number
US04054572

Reaction notes

Loading…