Chloroform methanol → HCID 70637790, compound

HRID 972949Notes

Reaction equation

HRID 972949 reaction equation
[CH3:1][N:2]([CH3:26])[CH:3]1[CH2:25][CH2:24][N:6]2[C:7]3[CH:19]=[C:18](C(F)(F)F)[CH:17]=[CH:16][C:8]=3S[C:10]3[CH:15]=[CH:14][CH:13]=[CH:12][C:11]=3[CH:5]2[CH2:4]1.[CH:27](Cl)(Cl)Cl.CO>>[CH3:1][N:2]([CH3:26])[CH:3]1[CH2:25][CH2:24][N:6]2[C:7]3[CH:19]=[CH:18][CH:17]=[CH:16][C:8]=3[CH2:27][C:10]3[CH:15]=[CH:14][CH:13]=[CH:12][C:11]=3[CH:5]2[CH2:4]1

Participants

3

Reactant 2

HCID 21584188Chloroform methanolHCID 70637564HCID 70637564, compound

Product 1

HCID 70637790HCID 70637790, compound

Procedure

2-dimethylamino-7-trifluoromethyl-1,3,4,14b-tetrahydro-2H-pyridino[ 1,2-d]-dibenzo[b,f](1,4)-thiazepine (2-equatorial), (oil); Rf = 0.45 in chloroform:methanol (8:2).

Sources & evidence

ORD record
ord-911a84522fff4e1baf3ebefdeb0b6f93
Source dataset
uspto-grants-1977_10
Patent number
US04054572

Reaction notes

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