Acetic Anhydride → 1-Acetoxy-2-(7-carbethoxyheptyl)cyclohex-1-ene

HRID 973014Notes

Reaction equation

[C:1]([CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH:13]1[CH2:18][CH2:17][CH2:16][CH2:15][C:14]1=[O:19])([O:3][CH2:4][CH3:5])=[O:2].[C:20](OC(=O)C)(=[O:22])[CH3:21]>>[C:20]([O:19][C:14]1[CH2:15][CH2:16][CH2:17][CH2:18][C:13]=1[CH2:12][CH2:11][CH2:10][CH2:9][CH2:8][CH2:7][CH2:6][C:1]([O:3][CH2:4][CH3:5])=[O:2])(=[O:22])[CH3:21]

Participants

Reactant 2

HCID 7918Acetic Anhydride

HCID 204655732-(7-Carbethoxyheptyl)cyclohexan-1-one

Product 1

HCID 204655341-Acetoxy-2-(7-carbethoxyheptyl)cyclohex-1-ene

Procedure

Treatment of 2-(7-carbethoxyheptyl)cyclohexan-1-one (Example 16) with acetic anhydride by the procedure of Example 24 is productive of the subject compound.

Sources & evidence

ORD record: ord-6502f5081fe04d3e910d548a0729dfa2
Source dataset: uspto-grants-1977_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04054604

Reaction notes

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