HRID973053

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID6371

Phosgene

CCl2O

HCID11658456

2-amino-4,6-dimethoxybenzoic acid

C9H11NO4

PRODUCTS

生成物

HCID11601010

4,6-dimethoxyisatoic anhydride

C10H9NO5

PROCEDURE

实验过程

4,6-Dimethoxyisatoic anhydride is prepared from 4,6-dimethoxyanthranilic acid (H. Newman & R. Anzier, J. Org. Chem. 34, 3484 (1969)) and phosgene according to the method of E. C. Wagner and M. F. Fegley, Org. Synthesis 27, 45 (1947).

WORKUP

后处理

customSynthesis 27, 45 (1947)