Acetic Acid → 4-n-Octyloxyphenacyl acetate

HRID 973085Notes

Reaction equation

HRID 973085 reaction equation
[CH2:1]([O:9][C:10]1[CH:19]=[CH:18][C:13]([C:14](=[O:17])[CH2:15]Br)=[CH:12][CH:11]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8].[C:20]([OH:23])(=[O:22])[CH3:21]>>[C:20]([O:23][CH2:15][C:14]([C:13]1[CH:18]=[CH:19][C:10]([O:9][CH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8])=[CH:11][CH:12]=1)=[O:17])(=[O:22])[CH3:21]

Participants

3

Reactant 2

HCID 176Acetic AcidHCID 134354532-Bromo-1-[4-(octyloxy)phenyl]ethan-1-one

Product 1

HCID 214035054-n-Octyloxyphenacyl acetate

Procedure

Following the procedure of Example 1, 5 grams of 4-n-octyloxyphenacyl bromide are reacted with 5 grams of acetic acid to obtain 4-n-octyloxyphenacyl acetate, m.p. 44°-45° C.

Sources & evidence

ORD record
ord-bbc0c6857c2a418f845e514a8e0653f6
Source dataset
uspto-grants-1977_10
Patent number
US04054719

Reaction notes

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