HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl chloride → HCID 12251780, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 178497612 | HCID 178497612 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 12251780 | HCID 12251780 | — |
Reaction Steps
A mixture of 30 g 3-(2-carbomethoxyphenyl)-5-(4-methoxyphenyl)pyrazole, 0.30 g sodium hydride and 0.8 g acetyl chloride in 50 ml anhydrous tetrahydrofuran (THF) is stirred and refluxed overnight. The reaction mixture is filtered and the THF is removed from the filtrate to yield 1-acetyl-3-(2-carbomethoxyphenyl)-5-(4-methoxyphenyl)-pyrazole.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04055409 |
| Source dataset | uspto-grants-1977_10 |
| ORD ID | ord-8194b6d978a7463383cd86a54143de0e |
| Source note | uspto-grants-1977_10 |