1-(Aminomethyl)cyclohexane-1-carboxylic acid → HCID 68118073, compound

HRID 973164Notes

Reaction equation

HRID 973164 reaction equation
[NH2:1][CH2:2][C:3]1([C:9]([OH:11])=[O:10])[CH2:8][CH2:7][CH2:6][CH2:5][CH2:4]1.[CH2:12](Cl)[CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19]/[CH:20]=[CH:21]\[CH2:22]/[CH:23]=[CH:24]\[CH2:25][CH2:26][CH2:27][CH2:28][CH3:29]>[OH-].[Na+]>[CH2:12]([NH:1][CH2:2][C:3]1([C:9]([OH:11])=[O:10])[CH2:8][CH2:7][CH2:6][CH2:5][CH2:4]1)[CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19]/[CH:20]=[CH:21]\[CH2:22]/[CH:23]=[CH:24]\[CH2:25][CH2:26][CH2:27][CH2:28][CH3:29]

Participants

4

Reactant 2

HCID 139843081-(Aminomethyl)cyclohexane-1-carboxylic acidHCID 15635185HCID 15635185, compound

Product 1

HCID 68118073HCID 68118073, compound

Reagents, catalysts & solvents 1

HCID 14798Sodium HydroxideSolvent

Procedure

5 grams of aminomethylcyclohexanecarboxylic acid were dissolved in 50 cm3 of 6% sodium hydroxide. This solution was stirred vigorously and maintained at 10° C while 10 grams of linoleyl chloride were added drop by drop. The stirring was maintained for 1 hour at ambient temperature. The precipitate obtained on centrifuging was washed twice with acetone and allowed to dry.

Workup

  1. additionwere added drop by drop
  2. customThe precipitate obtained on centrifuging
  3. washwas washed twice with acetone
  4. customto dry

Sources & evidence

ORD record
ord-c9be480e3a9e4256b6afafe5b7ff1316
Source dataset
uspto-grants-1977_10
Patent number
US04055580

Reaction notes

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