HCID 3736869, compound → HCID 178435352, compound

HRID 973175Notes

Reaction equation

HRID 973175 reaction equation
[NH2:1][CH:2]([C:4]1[CH:13]=[C:12]2[C:7]([C:8]([CH3:17])([CH3:16])[CH2:9][CH2:10][C:11]2([CH3:15])[CH3:14])=[CH:6][C:5]=1[CH2:18][CH3:19])[CH3:3].[ClH:20].C[CH:22]([NH2:37])[C:23]1C=[CH:27][C:26](CCC2C=CC=CC=2)=[CH:25][CH:24]=1>>[ClH:20].[CH2:18]([C:5]1[CH:6]=[C:7]2[C:12]([C:11]([CH3:15])([CH3:14])[CH2:10][CH2:9][C:8]2([CH3:17])[CH3:16])=[CH:13][C:4]=1[CH:2]([N:1]=[C:22]1[CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][NH:37]1)[CH3:3])[CH3:19]

Participants

3

Reactant 2

HCID 3736869HCID 3736869, compoundHCID 13012107alpha-Methyl-p-phenethylbenzylamine hydrochloride

Product 1

HCID 178435352HCID 178435352, compound

Procedure

Following essentially the same procedure described in Example IV above and substituting 7-(α-aminoethyl)-6-ethyl-1,1,4,4-tetramethyl-1,2,3,4-tetrahydronaphthalene for the α-methyl-ρ-phenethylbenzylamine hydrochloride above, results in the formation of 2-[1-(7-ethyl-1,2,3,4-tetrahydro-1,1,4,4-tetramethyl-6-naphthyl)ethylimino]hexahydro-1H-azepine hydrochloride, having a M.P. of 246.5°-7.5° C. (dec.)

Sources & evidence

ORD record
ord-8c2c86cd09d140878ceca61d40dfdaf3
Source dataset
uspto-grants-1977_10
Patent number
US04055561

Reaction notes

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