alpha-Methyl-p-phenethylbenzylamine hydrochloride → HCID 178463291, compound

HRID 973180Notes

Reaction equation

HRID 973180 reaction equation
Cl.[CH:2]1[C:14]2[C:13](=[CH:15][C:16]3[CH:24]=[CH:23][C:19]([CH:20]([NH2:22])[CH3:21])=[CH:18][CH:17]=3)[C:12]3[C:7](=[CH:8][CH:9]=[CH:10][CH:11]=3)[C:6]=2[CH:5]=[CH:4][CH:3]=1.Cl.C[CH:27]([NH2:42])[C:28]1C=[CH:32][C:31](CCC2C=CC=CC=2)=[CH:30][CH:29]=1>>[CH:11]1[C:12]2[C:13](=[CH:15][C:16]3[CH:17]=[CH:18][C:19]([CH:20]([N:22]=[C:27]4[CH2:28][CH2:29][CH2:30][CH2:31][CH2:32][NH:42]4)[CH3:21])=[CH:23][CH:24]=3)[C:14]3[C:6](=[CH:5][CH:4]=[CH:3][CH:2]=3)[C:7]=2[CH:8]=[CH:9][CH:10]=1

Participants

3

Reactant 2

HCID 13012107alpha-Methyl-p-phenethylbenzylamine hydrochlorideHCID 13012111HCID 13012111, compound

Product 1

HCID 178463291HCID 178463291, compound

Procedure

Following essentially the same procedure described in Example IV above and substituting ρ-(fluoren-9-ylidenemethyl)-α-methylbenzylamine hydrochloride for the α-methyl-ρ-phenethylbenzylamine hydrochloride above results in the formation of 2-[[1-[ρ-(fluoren-9-ylidenemethyl)phenyl]ethylimino]]-hexahydro-1H-azepine, having a M.P. of 265.5°-7.5° C. (dec.)

Sources & evidence

ORD record
ord-ff7f7a8bc76d470daaec03bd593487dc
Source dataset
uspto-grants-1977_10
Patent number
US04055561

Reaction notes

Loading…