HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Ether → HCID 178486632, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 178486646 | HCID 178486646 | — |
| Product | HCID 178486632 | HCID 178486632 | — |
Reaction Steps
A suspension of 2.00 g of N2 -(6,7-dimethoxy-2-naphthalenesulfonyl)-L-arginine in 20 ml of thionyl chloride was stirred for 2 hours at room temperature. Addition of cold dry diethyl ether resulted in a precipitate which was collected by filtration and washed several times with dry diethyl ether to give N2 -(6,7-dimethoxy-2-naphthalensulfonyl)-L-arginyl chloride hydrochloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04055636 |
| Source dataset | uspto-grants-1977_10 |
| ORD ID | ord-94f7070f55af43ca9a0b6ba3f4c84dd8 |
| Source note | uspto-grants-1977_10 |