HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diazomethane → HCID 13384290, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diazomethane | HCID 9550 | — |
| Reactant | HCID 13384291 | HCID 13384291 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 13384290 | HCID 13384290 | — |
Reaction Steps
A solution of (±)-2-(6-methoxy-2-naphthylmethoxy)-3,3,3-trifluoro-2-methylpropionic acid (1.0 g.) in ether is treated with diazomethane by the process described in Example 18 to give (±)-methyl 2-(6-methoxy-2-naphthylmethoxy)-3,3,3-trifluoro-2-methylpropionate (0.8 g.) m.p. 60°-62° C. (from methanol at -50° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04055595 |
| Source dataset | uspto-grants-1977_10 |
| ORD ID | ord-a5c438ddaf8d4c5795320f61ec39a6b6 |
| Source note | uspto-grants-1977_10 |