HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diazomethane → HCID 13384247, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diazomethane | HCID 9550 | — |
| Reactant | 3,3,3-Trifluoro-2-methyl-2-(4-phenoxyphenoxy)propanoic acid | HCID 13384248 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 13384247 | HCID 13384247 | — |
Reaction Steps
A solution of (±)-2-(4-phenoxyphenoxy)-3,3,3-trifluoro-2-methylpropionic acid (6.4 g.) in ether is treated with an excess of ethereal diazomethane at 0° C. The solution is evaporated and the residue distilled to give (±)-methyl 2-(4-phenoxyphenoxy)-3,3,3-trifluoro-2-methylpropionate (3.3 g.), b.p. 187° C. at 0.1 mm. pressure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04055595 |
| Source dataset | uspto-grants-1977_10 |
| ORD ID | ord-a83a437c40b84e11a48f23db69fd8eda |
| Source note | uspto-grants-1977_10 |