HRID973340

反应详情

EQUATION

反应方程式

HRID 973340 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

(4S)-4-(2-Tetrahydropyranyloxy)-2-nonynal (54.6 g., 0.23 mole) in dioxane (200 ml.) is hydrogenated at room temperature and a pressure of 2-3 atmospheres over a 5% palladium on charcoal catalyst to yield (4S)-4-(2-tetrahydropyranyloxy)nonanal purified by distillation at reduced pressure.

WORKUP

后处理

  1. customis hydrogenated at room temperature