HuagongsheHuagongshe Chemistry Print Report · For research reference only
118317-76-3 → Methyl N-(tert-butoxycarbonyl)-3-oxoserinate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 118317-76-3 | HCID 15018080 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Methyl N-(tert-butoxycarbonyl)-3-oxoserinate | HCID 11128196 | 107% |
Reaction Steps
BOC-NHCH(CO2Me)CO2CH2Ph (16.2 g) was dissolved in MeOH (250 ml), to which was added 20% Pd/C (0.66 g). The suspension was purged with H2 for 1.5 hours, filtered, and stripped at 30° in vacuo, giving a syrup (12.5 g) which was kept at 4° until use in the following step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05063207 |
| Source dataset | uspto-grants-1991_11 |
| ORD ID | ord-ca13b28abe8b408d8f28d2f3f284c832 |
| Source note | uspto-grants-1991_11 |