HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,4-Dihydroxybenzaldehyde → HCID 54039882, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,4-Dihydroxybenzaldehyde | HCID 8768 | — |
| Reactant | Cyanoacetic acid | HCID 9740 | — |
| Reactant | 3',4'-Dimethoxycinnamic acid | HCID 16848 | — |
| Reactant | Boron Trichloride | HCID 25135 | — |
| Reactant | 3-(3',4'-Dimethoxyphenyl)-1-propanol | HCID 77528 | — |
| Product | HCID 54039882 | HCID 54039882 | — |
Reaction Steps
After the reduction of 3,4-dimethoxycinnamic acid to 3-(3,4-dimethoxyphenyl)propanol in the usual manner followed by condensation with cyanoacetic acid according to the procedure in Example 3, the product was demethylated with boron trichloride and condensed with 3,4-dihydroxybenzaldehyde to give the following compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05063243 |
| Source dataset | uspto-grants-1991_11 |
| ORD ID | ord-e8db239b42e44e63874fdb8a7a81064e |
| Source note | uspto-grants-1991_11 |