Hydrogen Bromide → HCID 86745196, compound

Participants

Reaction Steps

The resultant compound from Example 73 (315 mg, 0.828 mmol) was stirred for 2 h in 30% HBr in acetic acid (5 ml). The solvent was evaporated and the residue was dissolved in water which was washed with ether and lyophillized to afford 310 mg (100%) of the desired product as a foam. 1H NMR (CD3OD) δ7.20-7.35 (m,5H), 6.72 (s,1H), 3.44 (s,3H), 3.08 (s,3H), 2.70-3.20 (m,5H).

Provenance & Evidence