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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 973635Generated: October 29, 2026

Hydrochloric Acid → HCID 10037816, compound

https://huagongshe.com/reaction/973635

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantHCID 10263800HCID 10263800—
ProductHCID 10037816HCID 10037816—

Reaction Conditions

Temperature80 °C

Reaction Steps

A mixture of 1.4 g (5.8 mMol) of ethyl 3-aminopropyl(1,1-difluorobutyl)phosphinate and 15 ml of 12M hydrochloric acid is stirred for 8 hours at 80° C. The reaction mixture is evaporated to dryness and the residue is recrystallized from ethanol/ether giving 3-aminopropyl(1,1-difluorobutyl)phosphinic acid hydrochloride, m.p. 149°-151° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05064819
Source datasetuspto-grants-1991_11
ORD IDord-a5db95e91f7f443c81e575026c7665c3
Source noteuspto-grants-1991_11