Thionyl Chloride → HCID 53685669, compound

HRID 973735Notes

Reaction equation

HRID 973735 reaction equation
[CH2:1]([C:4]1[CH:14]=[CH:13][C:12]([C:15]([F:18])([F:17])[F:16])=[CH:11][C:5]=1[O:6][CH2:7][C:8](O)=[O:9])[CH:2]=[CH2:3].S(Cl)([Cl:21])=O>>[CH2:1]([C:4]1[CH:14]=[CH:13][C:12]([C:15]([F:18])([F:17])[F:16])=[CH:11][C:5]=1[O:6][CH2:7][C:8]([Cl:21])=[O:9])[CH:2]=[CH2:3]

Participants

3

Reactant 2

HCID 24386Thionyl ChlorideHCID 53873723HCID 53873723, compound

Product 1

HCID 53685669HCID 53685669, compound

Procedure

Using the procedure of Step E of Example 16, 5.2 g of the product of Step B and 40 ml of thionyl chloride were reacted to obtain 5.55 g of the expected product which was used as is for Step D.

Workup

  1. customwere reacted

Sources & evidence

ORD record
ord-49ff5d7b8e184971a92d19c1072f19af
Source dataset
uspto-grants-1991_11
Patent number
US05064861

Reaction notes

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