Hydrochloric Acid → HCID 178469413, compound

Participants

Reaction Steps

The product obtained in Step 1 (4.1 g) and sodium hydrosulfide (2.6 g) were dissolved in 30 ml of water, the solution was refluxed for one hour, the reaction mixture was cooled to room temperature, its pH was lowered to 1.0 with 6N hydrochloric acid, and the colorless crystals thus formed were collected by filtration, giving 2.8 g of the objective compound.

Provenance & Evidence