HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine hydrate (1:1) → HCID 178428720, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | HCID 178429729 | HCID 178429729 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178428720 | HCID 178428720 | 87.9% |
Reaction Steps
The product obtained in Step 1 (3.0 g) was suspended in 30 ml of ethanol at room temperature. Hydrazine monohydrate (3.17 g) was added dropwise to this suspension and the mixture was refluxed for two hours. After cooling to room temperature, the formed crystals were collected by filtration and washed with 20 ml of ethanol, giving 2.6 g of the objective compound as red crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05064953 |
| Source dataset | uspto-grants-1991_11 |
| ORD ID | ord-64da4c2d07db460eac510cd8345484fe |
| Source note | uspto-grants-1991_11 |