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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 973884Generated: October 30, 2026

HCID 131716911, compound → HCID 54439078, compound

https://huagongshe.com/reaction/973884

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 131716911HCID 131716911—
SolventChloroform methanolHCID 21584188—
ProductHCID 54439078HCID 54439078—

Reaction Steps

The title compound was prepared from N-phthalyl-Phe (0.028 g, 95 μmol) and TFA-Leu-3-amino-4-cyclohexyl-2-hydroxy-butanoic acid methyl ester (81.7 μmol) following the procedure of Example 1, second paragraph. Column chromatography (SiO2 gel; 2% MeOH/CHCl3) yielded 0.036 g (73% yield) of pure compound with a diastereomeric ratio of 28:1.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05064965
Source datasetuspto-grants-1991_11
ORD IDord-f199ebe0ac9e486a9e50f6452e1c7369
Source noteuspto-grants-1991_11