Ammonia → HCID 591156, compound

HRID 974234Notes

Reaction equation

[CH3:1][C:2]1[C:11]2[C:10](=[O:12])[CH2:9][C:8]([CH3:14])([CH3:13])[CH2:7][C:6]=2[O:5][C:4](=O)[CH:3]=1.[NH3:16]>>[CH3:1][C:2]1[C:11]2[C:10](=[O:12])[CH2:9][C:8]([CH3:14])([CH3:13])[CH2:7][C:6]=2[NH:16][C:4](=[O:5])[CH:3]=1

Participants

Reactant 2

HCID 222Ammonia

HCID 2728740HCID 2728740, compound

Product 1

HCID 591156HCID 591156, compound

Procedure

Prepared from 4,7,7-trimethyl-5,6,7,8-tetrahydro- cumarin-5-one and methanolic ammonia analogously to Example C(b).

Sources & evidence

ORD record: ord-a9fee7bb28f647499c1878ae74c9e61b
Source dataset: uspto-grants-1991_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05068334

Reaction notes

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