Methacrylic Acid → HCID 12742313, compound

HRID 974237Notes

Reaction equation

HRID 974237 reaction equation
[NH2:1][C:2]1[CH2:7][CH2:6][CH2:5][C:4](=[O:8])[CH:3]=1.[C:9](O)(=[O:13])[C:10]([CH3:12])=[CH2:11]>>[CH3:11][CH:10]1[CH2:12][C:3]2[C:4](=[O:8])[CH2:5][CH2:6][CH2:7][C:2]=2[NH:1][C:9]1=[O:13]

Participants

3

Reactant 2

HCID 4093Methacrylic AcidHCID 788923-Aminocyclohex-2-en-1-one

Product 1

HCID 12742313HCID 12742313, compound

Procedure

Prepared analogously to Example G from 1-amino- cyclohexen-3-one and methacrylic acid in an autoclave for a period of one hour at 180° C. Recrystallisation is from methanol and subsequently from a mixture of ethyl acetate/ethanol (3:1).

Workup

  1. customRecrystallisation
  2. additionis from methanol and subsequently from a mixture of ethyl acetate/ethanol (3:1)

Sources & evidence

ORD record
ord-93a5a2fbb3f74e9395e174ccfadecf03
Source dataset
uspto-grants-1991_11
Patent number
US05068334

Reaction notes

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