Ammonia → HCID 15924260, compound

HRID 974245Notes

Reaction equation

HRID 974245 reaction equation
[CH2:1]([C:3]1[C:12]2[C:11](=[O:13])[CH2:10][CH2:9][CH2:8][C:7]=2[O:6][C:5](=O)[CH:4]=1)[CH3:2].[NH3:15]>>[CH2:1]([C:3]1[C:12]2[C:11](=[O:13])[CH2:10][CH2:9][CH2:8][C:7]=2[NH:15][C:5](=[O:6])[CH:4]=1)[CH3:2]

Participants

3

Reactant 2

HCID 222AmmoniaHCID 15924259HCID 15924259, compound

Product 1

HCID 15924260HCID 15924260, compound

Procedure

Prepared from 4-ethyl-5,6,7,8-tetrahydro-cumarin- 5-one (prepared from ethyl 3-oxo-n-valeriate and cyclohexan-1,3dione) and methanolic ammonia in an autoclave for 1 hour at 140° C.

Sources & evidence

ORD record
ord-7029e85a3926442eb6fe6c545c68b375
Source dataset
uspto-grants-1991_11
Patent number
US05068334

Reaction notes

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