Ammonia → HCID 15924263, compound

HRID 974247Notes

Reaction equation

HRID 974247 reaction equation
[CH3:1][C:2]1[C:3](=O)[O:4][C:5]2[CH2:6][CH2:7][CH2:8][C:9](=[O:13])[C:10]=2[C:11]=1[CH3:12].[NH3:15]>>[CH3:1][C:2]1[C:3](=[O:4])[NH:15][C:5]2[CH2:6][CH2:7][CH2:8][C:9](=[O:13])[C:10]=2[C:11]=1[CH3:12]

Participants

3

Reactant 2

HCID 222AmmoniaHCID 15924262HCID 15924262, compound

Product 1

HCID 15924263HCID 15924263, compound

Procedure

Prepared from 3,4-dimethyl-5,6,7,8-tetrahydro-cumarin- 5-one (melting point: 109°-111° C., prepared from methyl 2methylacetoacetate and cyclohexan-1,3-dione) and methanolic ammonia for one hour in an autoclave at 150° C.

Sources & evidence

ORD record
ord-c5d1c1eee8d7453183a739a22b17e9b4
Source dataset
uspto-grants-1991_11
Patent number
US05068334

Reaction notes

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