HRID974277

反应详情

EQUATION

反应方程式

REACTANTS

反应物

反应SMILES：COC(=O)C(=Cc1cccc([N+](=O)[O-])c1)C(C)=O

HCID1536427

Methyl 2-[(3-nitrophenyl)methylene]-3-oxobutanoate

C12H11NO5

$反应SMILES：COCCOC(=O)/C=C(\N)Cn1ccnc1$

HCID19986033

未命名化合物

PRODUCTS

产物

反应SMILES：COCCOC(=O)C1=C(Cn2ccnc2)NC(C)=C(C(=O)OC)C1c1cccc([N+](=O)[O-])c1

HCID67928278

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID702

Ethanol

C2H6O

PROCEDURE

实验过程

A mixture of methyl 2-(3-nitrobenzylidene)-acetoacetate (2.5 g, 0.01 mol), ethanol (20 ml) and 2-methoxyethyl 3-amino-4-(imidazol-1-yl)crotonate (3 g) is heated at reflux for 5 hours to give the title compound.

WORKUP

后处理

temperatureis heated
temperatureat reflux for 5 hours