HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Ether → HCID 54117733, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | 2-Amino-4,5,6,7,8-pentahydrothiazolo[5,4-d]azepine | HCID 19985785 | — |
| Reactant | HCID 54145400 | HCID 54145400 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 54117733 | HCID 54117733 | 13% |
Reaction Steps
Prepared from 4-benzyloxy-cinnamyl chloride and 2 equivalents of 2-amino-4,5,7,8-tetrahydro-6H- thiazolo[5,4-d]azepine in chloroform for one hour at 50° C. Yield: 13% of theory, Melting point: 135°-140° C. (ether).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05068325 |
| Source dataset | uspto-grants-1991_11 |
| ORD ID | ord-24a9457c3cff4c9884bc4101a109b444 |
| Source note | uspto-grants-1991_11 |