HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,3-Bis(4-fluorophenyl)-2-(2-ethyl-2H-tetrazol-5-yl)-2-propenol → 3,3-Bis(4-Fluorophenyl)-2-(2-ethyl-2H-tetrazol-5-yl)-2-propenal
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,3-Bis(4-fluorophenyl)-2-(2-ethyl-2H-tetrazol-5-yl)-2-propenol | HCID 14723824 | — |
| Reactant | HCID 178418287 | HCID 178418287 | — |
| Product | 3,3-Bis(4-Fluorophenyl)-2-(2-ethyl-2H-tetrazol-5-yl)-2-propenal | HCID 14723827 | 79.7% |
Reaction Steps
The reaction of 4.0 g (12.0 mmoles) of 3,3-bis(4-fluorophenyl)-2-(2-ethyl-2H-tetrazol-5-yl)-2-propenol with pyridinium chlorochromate (4.5 g) was carried out by the procedure described in Example 48 and there was thereby produced 3.25 g (79.7%) of the title compound; m.p.=138°-139° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05068346 |
| Source dataset | uspto-grants-1991_11 |
| ORD ID | ord-6fdc6386526c45c3832069b30d59c56e |
| Source note | uspto-grants-1991_11 |