HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 14724008, compound → HCID 14723828, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 14724008 | HCID 14724008 | — |
| Catalyst | HCID 178418406 | HCID 178418406 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 14723828 | HCID 14723828 | — |
Reaction Steps
To a solution of 2.2 g (4.0 mmol) 3,3-bis(4-fluorophenyl)-2-[2-(triphenylmethyl)-2H-tetrazol-5-yl]-2-propenol in 100 mL methylene chloride was added 7 g of activated manganese dioxide. After stirring the resultant mixture for 20 hours, the insolubles were removed by filtration and the filtrate concentrated in vacuo to give a quantitative yield of the title compound, m.p.=208° C. (dec).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05068346 |
| Source dataset | uspto-grants-1991_11 |
| ORD ID | ord-2fda606ac1e7447b93da44bef2d0b125 |
| Source note | uspto-grants-1991_11 |