Methyl Isocyanate → HCID 13420167, compound

HRID 974578Notes

Reaction equation

[F:1][C:2]([F:15])([F:14])[C:3]1[CH:13]=[CH:12][CH:11]=[CH:10][C:4]=1[O:5][CH:6]1[CH2:9][NH:8][CH2:7]1.[CH3:16][N:17]=[C:18]=[O:19]>>[CH3:16][NH:17][C:18]([N:8]1[CH2:9][CH:6]([O:5][C:4]2[CH:10]=[CH:11][CH:12]=[CH:13][C:3]=2[C:2]([F:1])([F:14])[F:15])[CH2:7]1)=[O:19]

Participants

Reactant 2

HCID 12228Methyl Isocyanate

HCID 128125053-[2-(Trifluoromethyl)phenoxy]azetidine

Product 1

HCID 13420167HCID 13420167, compound

Procedure

The compound was prepared from 3-[2-(trifluoromethyl)phenoxy]azetidine and methylisocyanate as described in Example 5 of U.S. Pat. No. 4,226,861, m.p. 134°-136° C.

Sources & evidence

ORD record: ord-305632c5062545c8bb586db723d8bc89
Source dataset: uspto-grants-1991_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05068231

Reaction notes

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