HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Benzyl-1-methyl-5,7-dioxooctahydropyrrolo[3,4-b]pyridine → 6-Benzyl-1-methyloctahydropyrrolo[3,4-b]pyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Benzyl-1-methyl-5,7-dioxooctahydropyrrolo[3,4-b]pyridine | HCID 15070007 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 6-Benzyl-1-methyloctahydropyrrolo[3,4-b]pyridine | HCID 15070008 | — |
Reaction Steps
19.2 g (0.08 mol) of crude 6-benzyl-1-methyl-5,7-dioxooctahydropyrrolo[3,4-b]pyridine are reduced with 6.1 g (0.16 mol ) of lithium aluminum hydride in absolute tetrahydrofuran in accordance with the working instructions of Example Ic.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05607942 |
| Source dataset | uspto-grants-1997_03 |
| ORD ID | ord-3e35bed580f049539b935bc5a99477fe |
| Source note | uspto-grants-1997_03 |