Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
N-allyl-N-(2,2-dimethoxypropyl)-acetamide → N-allyl-N-(2-oxopropyl)-acetamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | N-allyl-N-(2,2-dimethoxypropyl)-acetamide | HCID 15069990 | — |
| 용매 | Formic Acid | HCID 284 | — |
| 생성물 | N-allyl-N-(2-oxopropyl)-acetamide | HCID 15069994 | — |
반응 단계
85.5 g (0.425 mol) of N-allyl-N-(2,2-dimethoxypropyl)-acetamide are heated under reflux with 212 ml of formic acid for one hour. The mixture is poured onto 500 g of ice and extracted several times with methylene chloride, the organic phases are washed with sodium bicarbonate solution, dried over magnesium sulphate and concentrated and the residue is distilled.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05607942 |
| 출처 데이터셋 | uspto-grants-1997_03 |
| ORD ID | ord-f4177a087bc1470d9ff09325d68951b4 |
| 출처 메모 | uspto-grants-1997_03 |