HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl chloroformate → Ethyl 7-benzyl-2,7-diazabicyclo[3.3.0]octane-2-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl chloroformate | HCID 10928 | — |
| Reactant | HCID 19969795 | HCID 19969795 | — |
| Product | Ethyl 7-benzyl-2,7-diazabicyclo[3.3.0]octane-2-carboxylate | HCID 15070027 | — |
Reaction Steps
Ethyl 2,7-diazabicyclo[3.3.0]octane-2-carboxylate 7-Benzyl-2,7-diazabicyclo[3.3.0]octane (Example Jc) is reacted with ethyl chloroformate analogously to Example Oa) to give ethyl 7-benzyl-2,7-diazabicyclo[3.3.0]octane-2-carboxylate, and this is then debenzylated hydrogenolyrically analogously to Example Jd). A colorless oil of boiling point 90° C./0.1 mbar is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05607942 |
| Source dataset | uspto-grants-1997_03 |
| ORD ID | ord-922bcda4177b40cea8d03ec79e614adc |
| Source note | uspto-grants-1997_03 |