HCID 53738665, compound → HCID 22870338, compound

HRID 975136Notes

Reaction equation

HRID 975136 reaction equation
[OH:1][CH:2]([CH3:22])[CH2:3][CH:4]=[CH:5][C:6]1[CH:7]=[C:8]2[C:12](=[CH:13][CH:14]=1)[NH:11][CH:10]=[C:9]2[CH2:15][C@H:16]1[CH2:20][CH2:19][CH2:18][N:17]1[CH3:21]>[Pd].O>[OH:1][CH:2]([CH3:22])[CH2:3][CH2:4][CH2:5][C:6]1[CH:7]=[C:8]2[C:12](=[CH:13][CH:14]=1)[NH:11][CH:10]=[C:9]2[CH2:15][C@H:16]1[CH2:20][CH2:19][CH2:18][N:17]1[CH3:21]

Participants

4

Reactant 1

HCID 53738665HCID 53738665, compound

Product 1

HCID 22870338HCID 22870338, compound

Reagents, catalysts & solvents 2

HCID 23938PalladiumCatalystHCID 962WaterSolvent

Procedure

Obtained from the title compound of Example 15 by a procedure similar to that described in Example 2, but using 10% palladium on charcoal as catalyst, as a foam. Rf 0.16 (SS 7). Found: C,75.18; H,8.91; N,9.07. C19H28N2O; 0.17 H2O requires C,75.19; H,9.41; N,9.22%.

Sources & evidence

ORD record
ord-cdbf034a3f4e4211aec8ad5c08ce54db
Source dataset
uspto-grants-1997_03
Patent number
US05607960

Reaction notes

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