HRID975140

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID317028

vinylcyclopentanol

C7H12O

结构：O=C(OCc1ccccc1)N1CCC[C@@H]1Cc1c[nH]c2ccc(Br)cc12

HCID22859561

未命名化合物

PRODUCTS

生成物

结构：O=C(OCc1ccccc1)N1CCC[C@@H]1Cc1c[nH]c2ccc(C=CC3(O)CCCC3)cc12

HCID54322244

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID887

Methanol

CH4O

PROCEDURE

实验过程

Obtained by a procedure similar to that described in Example 1, from 3-(N-benzyloxycarbonyl-2(R)-pyrrolidinylmethyl)-5-bromo-1H-indole (Preparation 1) and 1-vinylcyclopentanol (Example 5(a)), as a foam. Rf 0.40 (SS 10). [α]D25 -31° (c=0.1, CH3OH). Found: C,75.58; H,7.24; N,6.22. C28H32N2O3 requires C,75.64; H,7.26; N,6.30%.

WORKUP

后处理

customObtained by a procedure similar to