HCID 54402989, compound → HCID 19970964, compound

HRID 975146Notes

Reaction equation

HRID 975146 reaction equation
[OH:1][C:2]1([CH:7]=[CH:8][C:9]2[CH:10]=[C:11]3[C:15](=[CH:16][CH:17]=2)[NH:14][CH:13]=[C:12]3[CH:18]2[CH2:23][CH2:22][N:21]([CH3:24])[CH2:20][CH2:19]2)[CH2:6][CH2:5][CH2:4][CH2:3]1>C(Cl)Cl>[OH:1][C:2]1([CH2:7][CH2:8][C:9]2[CH:10]=[C:11]3[C:15](=[CH:16][CH:17]=2)[NH:14][CH:13]=[C:12]3[CH:18]2[CH2:19][CH2:20][N:21]([CH3:24])[CH2:22][CH2:23]2)[CH2:6][CH2:5][CH2:4][CH2:3]1

Participants

3

Reactant 1

HCID 54402989HCID 54402989, compound

Product 1

HCID 19970964HCID 19970964, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

Obtained from the title compound of Example 44, by analogy with Example 43. Rf 0.40 (SS 7). Found: C,73.55; H,8.90; N,8.12. C21H30N2O; 0.25 CH2Cl2 requires C,73.44; H,8.85; N,8.06%.

Sources & evidence

ORD record
ord-f375f2feb5e3423694454b0b9e295ac4
Source dataset
uspto-grants-1997_03
Patent number
US05607960

Reaction notes

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