HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → 9H-Carbazole-9-propanenitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Carbazole | HCID 6854 | — |
| Reactant | Acrylonitrile | HCID 7855 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | 9H-Carbazole-9-propanenitrile | HCID 219300 | 42% |
Reaction Steps
Carbazole (8.0 g) was suspended in 100 ml of toluene, and 4 ml of acrylonitrile and subsequently 0.5 ml of Triton B were added to the suspension, whereby the suspension was solidified. Then, the reaction mixture was allowed to stand for one hour, and methanol was added thereto, followed by filtration to give 4.41 g (42%) of the product as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05607955 |
| Source dataset | uspto-grants-1997_03 |
| ORD ID | ord-c7224b8c88c74e579200fc4eae386458 |
| Source note | uspto-grants-1997_03 |