HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 86749440, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | (5-Iodothiophen-2-yl)methanol | HCID 14296055 | — |
| Product | HCID 86749440 | HCID 86749440 | — |
Reaction Steps
2-hydroxymethyl-5-iodothiophene was refluxed with Cu powder in dimethyl formamide ("DMF"). This Ullmann condensation also yielded a very low amount of 2,5-dihydroxymethyl bithiophene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05608081 |
| Source dataset | uspto-grants-1997_03 |
| ORD ID | ord-08f175b84ee94ca3ae0756b26240792b |
| Source note | uspto-grants-1997_03 |