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HRID975675

反应详情

EQUATION

反应方程式

HRID 975675 的结构方程式

REACTANTS

反应物

2
结构：NC(=O)c1ncc[nH]1
HCID133520

1H-Imidazole-2-carboxamide

C4H5N3O

结构：C=CCOC(=O)N1C[C@H](OS(C)(=O)=O)C[C@H]1CCOS(C)(=O)=O
HCID15537962

未命名化合物

PRODUCTS

生成物

1
结构：C=CCOC(=O)N1C[C@H](OS(C)(=O)=O)C[C@H]1CCn1ccnc1C(N)=O
HCID54523979

未命名化合物

收率 68%

PROCEDURE

实验过程

(2R,4R)-1-Allyloxycarbonyl-4-methylsulfonyloxy-2-(2-methylsulfonyloxyethyl) pyrrolidine (21.5 g) and 2-carbamoylimidazole (7.07 g) were reacted in substantially the same manner as that of Preparation 10-3) to give (2R,4R)-1-allyloxycarbonyl-2-{2-(2-carbamoylimidazol-1-yl) ethyl}-4-methylsulfonyloxypyrrolidine (15.2 g) as a yellow solid.

WORKUP

后处理

  1. customof Preparation 10-3)