HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 22099893, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 22099647 | HCID 22099647 | — |
| Product | HCID 22099893 | HCID 22099893 | — |
Reaction Steps
A mixture of 4.5 g of 6-[(2-methylbenzeneacetyl)amino]pyridine-3-carboxylic acid and 17 ml of thionyl chloride is heated on a steam bath for 1/2 hour. An additional 815 ml of thionyl chloride is added and the mixture refluxed for 0.5 hour. The volatiles are removed under vacuum and toluene (20 ml) added (twice) and the solvent removed under vacuum to give 5.3 g of a dark colored solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05610156 |
| Source dataset | uspto-grants-1997_03 |
| ORD ID | ord-d909c9815b8a40d58d393d0663b17c54 |
| Source note | uspto-grants-1997_03 |