HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 23698996, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Methyl 4-[[2-(Phenylmethyl)benzoyl]amino]benzoate | HCID 8765094 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 23698996 | HCID 23698996 | — |
Reaction Steps
A mixture of 4.90 g of methyl 4-[[2-(phenylmethyl)benzoyl]amino]benzoate in 100 ml of absolute ethanol and 3.50 ml of 10N sodium hydroxide is heated on a steam bath for 3 hours. The aqueous phase is filtered and the resulting solid collected and dried to give 4.25 g of the desired product m.p. 340°-346° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05610156 |
| Source dataset | uspto-grants-1997_03 |
| ORD ID | ord-267fc39348414e24beec36708a7eb6e7 |
| Source note | uspto-grants-1997_03 |