HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → 4-[[2-(Phenylmethyl)benzoyl]amino]benzoic Acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | HCID 23698996 | HCID 23698996 | — |
| Solvent | Water | HCID 962 | — |
| Product | 4-[[2-(Phenylmethyl)benzoyl]amino]benzoic Acid | HCID 22099697 | 100% |
Reaction Steps
A mixture of 4.0 g sodium 4-[[2-(phenylmethyl)benzoyl]amino]benzoate is suspended in water and the pH adjusted to 5 with acetic acid. The solid is collected by filtration and dried at 80° C. in vacuo to give 3.75 g of the desired product, 246°-247° C. M+ =332.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05610156 |
| Source dataset | uspto-grants-1997_03 |
| ORD ID | ord-290e2f5d64544f0ba6a59cfd06c63038 |
| Source note | uspto-grants-1997_03 |