HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Hydroxide → HCID 15788474, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | HCID 54179311 | HCID 54179311 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 15788474 | HCID 15788474 | 11.7% |
Reaction Steps
By proceeding in a fashion similar to that described in Example 9, but starting from 10.6 g of methyl cis-3-{3-[2-(2,5-diphenyl-1-pyrrolidinyl)-2-oxoethyl]ureido}phenylacetate in solution in 150 cm3 of methanol and 1.7 g of potassium hydroxide dissolved in 30 cm3 of water and after treatment and recrystallization in ethanol, 1.2 g of cis-3-{3-[2-(2,5-diphenyl-1-pyrrolidinyl)-2-oxoethyl]ureido}phenylacetic acid, melting at 152° C., are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05610144 |
| Source dataset | uspto-grants-1997_03 |
| ORD ID | ord-bda705e7da734339ae5032f510328a1f |
| Source note | uspto-grants-1997_03 |