HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 19968963, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 15293862 | HCID 15293862 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 19968963 | HCID 19968963 | — |
Reaction Steps
272 mg (0.515 mmol) of the compound of Example 60 was added to 10 ml of tetrahydrofuran. 2 ml of concentrated hydrochloric acid was added to the mixture and stirred at room temperature for 3 h. The solvent was distilled off under reduced pressure and the residue was recrystallized from ethanol to obtain 159 mg of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05610304 |
| Source dataset | uspto-grants-1997_03 |
| ORD ID | ord-f85dd5674efe4a49b479b691b4ea816a |
| Source note | uspto-grants-1997_03 |