HCID 19966842, compound → 3-Phenylpropylamine

HRID 976240Notes

Reaction equation

HRID 976240 reaction equation
C([C:4]1[CH:5]=[C:6]2[C:14](=[CH:15][CH:16]=1)NC1CC[CH:9]([N:17]3C(=O)C4=CC=CC=C4C3=O)[CH2:8][C:7]2=1)(O)=O.[N+](C1C=CC(C=CCN)=CC=1)([O-])=O>>[C:6]1([CH2:7][CH2:8][CH2:9][NH2:17])[CH:14]=[CH:15][CH:16]=[CH:4][CH:5]=1

Participants

3

Reactant 2

HCID 19966842HCID 19966842, compoundHCID 54076172HCID 54076172, compound

Product 1

HCID 162593-Phenylpropylamine

Procedure

Using 6-carboxy-3-phthalimido-1,2,3,4-tetrahydrocarbazole (0.60 g) and 3-(4-nitrophenyl)prop-2-enyl amine (0.32 g) (N. J. Malek and A. E. Moorman J. Org. Chem. 1982, 47, 5395) instead of 3-phenylpropylamine in the method of Example 1(b) gave, after recrystallisation from methanol/diethyl ether, the title compound (0.045 g) m.p. 139°-141° C. M/Z: C22H22N4O3 =391 (M+1)+.

Sources & evidence

ORD record
ord-ff776a2aecb44c938c810ea832d08ffa
Source dataset
uspto-grants-1997_03
Patent number
US05612331

Reaction notes

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