HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Nitrobenzenesulfonyl chloride → HCID 15338126, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Nitrobenzenesulfonyl chloride | HCID 7404 | — |
| Reactant | N-ISOBUTYL-2-PROPEN-1-AMINE | HCID 11062339 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 15338126 | HCID 15338126 | — |
Reaction Steps
To N-iso-Butyl-allylamine (11) (5 mmol) in pyridine (50 mL) at 55°-65° C. is added slowly 4-nitrobenzenesulfonyl chloride (12) (5.1 mmol). The mixture is allowed to stir for 4-6 hours at 55°-65° C. and the pyridine is then removed in vacuo and the residue purified by flash chromatography to afford N-allyl-N-iso-butyl-4-nitrobenzenesulfonamide (13).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05612339 |
| Source dataset | uspto-grants-1997_03 |
| ORD ID | ord-d1a43a5b9ea34bf2af4e9386579af9bb |
| Source note | uspto-grants-1997_03 |