Methylhydrazine → HCID 11743328, compound

Participants

Reaction Steps

4.5 g of methyl 4-(3,4,5,6,7,8-hexahydro-5,5,8,8-tetramethyl-1(2H)-anthracenon-2-ylcarbonyl)benzoate was suspended in 100 ml of methanol, followed by the addition thereto of 0.64 g of monomethylhydrazine. The obtained mixture was heated under reflux for 2 hours and cooled by allowing to stand to precipitate a solid. This solid was recovered by filtration and washed with methanol. 3.0 g of the title compound was obtained as a pale-yellow solid.

Provenance & Evidence