HuagongsheHuagongshe Chemistry Print Report · For research reference only
4H-Furo[2,3-e]pyrrolo[1,2-a][1,4]diazepine → 9,10-Dihydro-4H-furo[2,3-e]pyrrolo[1,2-a][1,4]diazepine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4H-Furo[2,3-e]pyrrolo[1,2-a][1,4]diazepine | HCID 11819471 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 9,10-Dihydro-4H-furo[2,3-e]pyrrolo[1,2-a][1,4]diazepine | HCID 21836966 | — |
Reaction Steps
A solution of 1 mmol of 4H-furo[2,3-e]pyrrolo[1,2-a][1,4]diazepine and 0.2 g of 10% Pd/C in 10 ml of ethanol is hydrogenated for 18 hours. The reaction mixture is filtered through diatomaceous earth and the filtrate is evaporated in vacuo to give the desired product as a solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05612334 |
| Source dataset | uspto-grants-1997_03 |
| ORD ID | ord-1200c09a1ed240d3bd7f00126486834e |
| Source note | uspto-grants-1997_03 |