HuagongsheHuagongshe Chemistry Print Report · For research reference only
o-Benzylbenzoic acid → 2-Benzylbenzoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | o-Benzylbenzoic acid | HCID 11924 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Product | 2-Benzylbenzoyl chloride | HCID 12682362 | — |
Reaction Steps
A mixture of 5.0 g of 2-(phenylmethyl) benzoic acid in 5.0 ml of thionyl chloride is heated on a steam bath for 1 hour. The volatiles are evaporated in vacuo to give 5.74 g of the desired product as an oil. M+ =227 as methyl ester.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05612334 |
| Source dataset | uspto-grants-1997_03 |
| ORD ID | ord-df4fc48fb9a243858230fde446b78d44 |
| Source note | uspto-grants-1997_03 |